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FilmTek™ 4000

Multiple Angle Reflectometry

 

FilmTek™ 4000 is our most advanced model for thick-film applications.  It incorporates multiple detectors positioned at different angles of incidence — plus our patented multi-angle Differential Power Spectral Density analysis capability — to accurately measure the index of refraction with a resolution of 0.00002.  That's 100 times the performance of the best non-contact method, 10 times that of the best prism coupler contact systems.  Additionally, the FilmTek™ 4000 can measure birefringence of anisotropic materials.  With the hot plate option, the index of refraction and thermal expansion of a film can be characterized as a function of temperature.  A prime application for this system is measuring the index of refraction and thickness of planar waveguide films.  The addition of the spectroscopic ellipsometer (SE) option extends the FilmTek™ 4000 measurement capability down to very thin films as well.  The FilmTek™ 4500 adds transmission measurement capability for transparent samples.  The FilmTek™ 4000 is available in a variety of configurations ranging from table-top systems suitable for R&D to fully automated, standalone production tools.

 

 

FilmTek™ 4000

 

 

FilmTek™ 4000-A

 

 

FilmTek™ 4500SE

 

 

FilmTek™ 4000SE

300mm Autoloader

 

FilmTek™ 4000 High Precision Measurement of Index

This unique FilmTek™ 4000 capability employ’s our patented DPSD (Differential Power Spectral Density) technique.  Spectroscopic reflection data are gathered at normal incidence and 70 degrees.  PSD processing results in two peaks in the Power Spectral Density domain.  The ratio of their positions is a function of the index of refraction of the film, and the angle of incidence of the oblique measurement.  This ratio is used to calculate the index.  Once the index is known, the thickness can be calculated from the optical thickness of the normal incident peak.

 

Differential Power Spectral Density analysis of an oxide film.

 

Index Map @ 1550nm of a doped oxide

 measured with FilmTek™ 4000.

 

FilmTek™ 4000 Features

Versatile: FilmTek™ 4000 incorporates SCI’s generalized material model with advanced global optimization algorithms for simultaneous determination of:

 

- Multiple layer thicknesses from 1Ĺ to 350µm
- Optical properties from 190nm-1700nm
- TE and TM indices of refraction [ n(l ) ]
- Extinction (absorption) coefficients [ k(l ) ]
- Energy band gap [ Eg ]        
- Constituent and void fraction
- Surface roughness
No Special Knowledge Required: FilmTek™ 4000 software is designed so that minimal experience in personal computers, thin film optical design, or measurement techniques is required.
Complete "turn key" System: A fully integrated spectrophotometer measurement system with calibration, acquisition, and analysis software.
Non-contact and non-destructive.
Flexible: FilmTek™ 4000 hardware and software can be easily modified to satisfy unique customer requirements.
Optional features:
- Spectroscopic ellipsometry option for thin films (rotating compensator design)
- Cassette to cassette wafer handling
- Heating/cooling chuck
- 300mm, FOUP, and SMIF compatible

 

 SiO2 Film Properties vs Temperature

Measured by FilmTek™ 4000 with heating chuck during one heat-cool cycle.

 

Applications

Virtually all translucent films ranging in thickness from 1 angstrom to approximately 250 microns can be measured with high precision. Typical applications include:


Semiconductor and dielectric materials Computer disks
Multilayer optical coatings Coated glass
Optical antireflection coatings Laser mirrors
Electro-optical materials Thin Metals


Example Films

SiOx a-Si
SiNx a-C:H
DLC ITO
SOG         Polysilicon
Photoresist Polyimide
Thin Metals Low K Dielectric Films


Example Substrates

Silicon GaAs
SOI Glass
SOS Aluminum

 

Technical Specifications

Film thickness range:

1Ĺ to 350µm (3nm to 250µm is standard)

Index resolution

2x10-5

Wide spectral range:

190 to 1700nm (380 to 1000nm is standard)

Spectral resolution:

0.3-2nm

 

Methodology

FilmTek™ simultaneously solves for refractive index n(l), extinction coefficient k(l), and thicknesses of multi-layer film structures.  A self-consistent solution is obtained by using SCI’s generalized dispersion formula to model fitted values of the dielectric function e (l).  The SCI dispersion formula is quite general and applies to metallic, amorphous, crystalline, and dielectric materials (Figures 1-3).  This approach allows the user to model complex multi-layer structures with reflection/transmission data.  Global optimization methods are used to obtain the best solution while avoiding local minima and minimizing sensitivity to the user’s initial guess of fitted parameters (e.g., layer thickness).  FilmTek™ optimizes both the reflectance and power density spectrum (FFT) simultaneously.  This unique feature allows for accurate thickness determination over a wide range of thickness (1Ĺ to 350µm).

 

 

 
Fig. 1 n and k spectra of Silicon
 
Fig. 2 n and k spectra of SiO2
 
Fig. 3 n and k spectra of Tantalum

Related Information

FilmTek™ 4000 Product Overview.pdf

 
 

 

 

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